Liu, Shengping published the artcileNickel-catalyzed oxidative dehydrogenative coupling of alkane with thiol for C(sp3)-S bond formation, SDS of cas: 4410-99-5, the publication is Tetrahedron Letters (2021), 152950, database is CAplus.
A nickel-catalyzed oxidative dehydrogenative coupling reaction of alkanes RH (R = 1-phenylethan-1-yl, cyclohexyl, tetrahydrofuran-2-yl, 1,4-dioxan-2-yl, etc.) with thiols R1SH (R1 = 4-methylphenyl, 2-naphthyl, octan-1-yl, benzo[d]thiazol-2-yl, etc.) for the construction of C(sp3)-S bond has been established, affording more than 50 alkyl thioethers RSR1. Notably, pharmaceutical and agrochems., such as Provigil, Chlorbenside and Pyridaben, were readily synthesized by this approach. The sterically hindered ligand bathocuproine (BC) and disulfide which was formed in situ oxidation of thiol, efficiently avoiding nickel-catalyst poisoning. A set of mechanistic experiments disclose both Ni-catalyzed and Ni-free HAA processes.
Tetrahedron Letters published new progress about 4410-99-5. 4410-99-5 belongs to alcohols-buliding-blocks, auxiliary class Thiol,Benzene, name is 2-Phenylethanethiol, and the molecular formula is C8H10S, SDS of cas: 4410-99-5.
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