Ido, Yohei published the artcileA Reactor System Using Electrospray in the Liquid Phase and Its Application in Selective Cyclosiloxane Synthesis, Quality Control of 597-52-4, the publication is Industrial & Engineering Chemistry Research (2017), 56(16), 4878-4882, database is CAplus.
Electrospraying is an electrochem. technique in which fine droplets are generated in the balance of electrostatic repulsion and surface tension. In this paper, we applied electrospray in the liquid phase in a new reactor system in which pos. and neg. charged fine droplets collided with each other between two electrospray nozzles submerged in a solvent. When the hydrolysis of alkylchlorosilanes was carried out using this reactor, not only did the reaction rates increase, but also, the product distribution changed: the kinetically favored cyclotrimer was predominantly formed over the thermodynamically favored cyclotetramer. The yield of cyclotrimer increased with an increase in the voltage between the needles. Since the droplet size decreases with an increase in the applied voltage, the result suggests that the formed cyclotrimer could diffuse into the solvent before it was converted to the thermodynamically favored cyclotetramer.
Industrial & Engineering Chemistry Research published new progress about 597-52-4. 597-52-4 belongs to alcohols-buliding-blocks, auxiliary class Aliphatic Chain, name is Triethylsilanol, and the molecular formula is C6H16OSi, Quality Control of 597-52-4.
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