Pearl, Irwin A. published the artcileLignin and related products. XVI. Synthesis of lignin model compounds of the phenylglycerol β-ether and related series, SDS of cas: 70110-65-5, the publication is Journal of Organic Chemistry (1962), 2111-14, database is CAplus.
Substituted ethyl benzoylacetates have been employed for the preparation of lignin model compounds in the phenylpropane-1,3-diol and phenylpropane-1,2,3-triol series. Direct reduction of these esters with LiAlH4 yields the corresponding phenylpropane-1,3-diol. Bromination followed by condensation with a phenol and reduction with LiAlH4 of the resulting ether yields the phenylglycerol β-aryl ether. Bromination followed by acetylation and reduction yields the phenylpropane-1,2,3-triol. Models in the veratryl, 3,4,5-trimethoxyphenyl, 4-hydroxy-3,5-dimethoxyphenyl, 4-benzyloxy-3,5-dimethoxyphenyl, and 4-acetoxy-3,5-dimethoxyphenyl series were prepared Cf. Forest Prod. J. 11, 442(1961); CA 54, 385f.
Journal of Organic Chemistry published new progress about 70110-65-5. 70110-65-5 belongs to alcohols-buliding-blocks, auxiliary class Benzene,Alcohol,Ether,Benzene Compounds, name is 2-Phenoxy-1-phenylpropane-1,3-diol, and the molecular formula is C15H16O3, SDS of cas: 70110-65-5.
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