Dem’yanov, I. N. published the artcileVinyltrimethylene and its Derivatives, Category: alcohols-buliding-blocks, the publication is Zhurnal Russkago Fiziko-Khimicheskago Obshchestva (1913), 176-84, database is CAplus.
The alc. (a) obtained by shaking vinyltrimethylene (b) with H2SO4 (Gustavson, J. prakt. Chem., [2] 54, 104), not being oxidizable to an aldehyde or ketone, is doubtless tertiary; it b755, 117.5-8.5° m. -5°, d422 0.889, n422 1.4315. Of the 2 formulas of (a), and preference is given to the 2nd. By converting (a) into an iodide (b22 50°) and treating the latter with Zn + AcOH a mixture of a hydrocarbon C5H10 (c) and the acetate of (a) was obtained. (c) b753 34-5°, d00 0.6973, d40 0.6805, nD17 1.3814; its formula is supposed to be. A hydrocarbon almost identical with (c) is more readily obtainable by reducing (b) with H + Pt black. The acetate of (c) b. 130-2.5°, d420 0.9351, nD20 1.419.
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva published new progress about 20117-47-9. 20117-47-9 belongs to alcohols-buliding-blocks, auxiliary class Aliphatic cyclic hydrocarbon,Alcohol, name is 1-Methylcyclobutan-1-ol, and the molecular formula is C5H10O, Category: alcohols-buliding-blocks.
Referemce:
https://en.wikipedia.org/wiki/Alcohol,
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