Spell, Mark L. published the artcileA Visible-Light-Promoted O-Glycosylation with a Thioglycoside Donor, Quality Control of 85618-21-9, the publication is Angewandte Chemie, International Edition (2016), 55(22), 6515-6519, database is CAplus and MEDLINE.
Visible-light irradiation of 4-p-methoxyphenyl-3-butenylthioglucoside donors in the presence of Umemoto’s reagent and alc. acceptors serves as a mild approach to O-glycosylation. Visible-light photocatalysts are not required for activation, and alkyl- and arylthioglycosides not bearing the p-methoxystyrene are inert to these conditions. Exptl. and computational evidence for an intervening electron donor-acceptor complex, which is necessary for reactivity, is provided. Yields with primary, secondary, and tertiary alc. acceptors range from moderate to high. Complete β-selectivity can be attained through neighboring-group participation.
Angewandte Chemie, International Edition published new progress about 85618-21-9. 85618-21-9 belongs to alcohols-buliding-blocks, auxiliary class Tetrahydropyran,Chiral,sulfides,Alcohol, name is (2R,3S,4S,5R,6S)-2-(Hydroxymethyl)-6-(octylthio)tetrahydro-2H-pyran-3,4,5-triol, and the molecular formula is C8H7N3, Quality Control of 85618-21-9.
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