Marciniec, Bogdan published the artcileSynthesis, first structures, and catalytic activity of the monomeric rhodium(I)-siloxide phosphine complexes, Product Details of C9H22OSi, the publication is Canadian Journal of Chemistry (2003), 81(11), 1292-1298, database is CAplus.
Four new square-plane rhodium siloxide complexes of the general formula [Rh(cod)(PR3‘)(OSiR3)] (R = Me, i-Pr, O-t-Bu, R’ = Cy, Ph) were synthesized and the structures of three of them were resolved by the x-ray method. [Rh(cod)(PCy3)(OSiMe3)] (1) appeared to be a very efficient catalyst for hydrosilylation of allyl glycidyl ether to yield, selectively, 3-glycidoxypropyltriethoxysilane, a com. important silane coupling agent. Catalytic measurements and stoichiometric experiments of 1 with triethoxysilane suggest a mechanism where an unsaturated Rh-H species is responsible for the catalysis.
Canadian Journal of Chemistry published new progress about 17877-23-5. 17877-23-5 belongs to alcohols-buliding-blocks, auxiliary class Protection and Derivatization Reagent, name is Triisopropylsilanol, and the molecular formula is C9H22OSi, Product Details of C9H22OSi.
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