Loska, Rafal published the artcileA three-component synthesis of aryl(heteroaryl)acylamides, Safety of 4,4-Diethoxybutan-1-amine, the publication is Organic & Biomolecular Chemistry (2015), 13(38), 9872-9882, database is CAplus and MEDLINE.
A three-component reaction of azole or azine N-oxides, 1,1-difluorostyrenes and amines gives amides of α-aryl-α-heteroarylacetic or propionic acids. The key step is 1,3-dipolar cycloaddition between N-oxide and difluorostyrene leading to the acyl fluoride intermediate, which has been identified and characterized by NMR spectroscopy. The whole process is an example of selective functionalization of C-H bonds in both 5- and 6-membered heterocyclic systems.
Organic & Biomolecular Chemistry published new progress about 6346-09-4. 6346-09-4 belongs to alcohols-buliding-blocks, auxiliary class Amine,Aliphatic hydrocarbon chain,Ether, name is 4,4-Diethoxybutan-1-amine, and the molecular formula is C8H19NO2, Safety of 4,4-Diethoxybutan-1-amine.
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