Furkert, Daniel P. published the artcileNonsymmetrical Azocarbonamide Carboxylates as Effective Mitsunobu Reagents, Related Products of alcohols-buliding-blocks, the publication is European Journal of Organic Chemistry (2014), 2014(35), 7806-7809, database is CAplus.
The nonsym. Mitsunobu reagents possessing both dialkyl amide and ester substituents was developed. These new reagents were readily prepared in a single pot from inexpensive, com. available materials by using a scalable and environmentally friendly procedure. They were shown to exhibit activity parallel to that of di-Et azodicarboxylate/diisopropyl azodicarboxylate in a wide variety of Mitsunobu reactions. Importantly, the acyl hydrazine reaction byproducts were readily separable from the crude mixture by standard aqueous workup. In addition, the discovery of effective nonsym. Mitsunobu reagents offers new directions for the ongoing development of this important reaction.
European Journal of Organic Chemistry published new progress about 57044-25-4. 57044-25-4 belongs to alcohols-buliding-blocks, auxiliary class Epoxides,Chiral,Aliphatic hydrocarbon chain,Alcohol, name is (R)-Oxiran-2-ylmethanol, and the molecular formula is C3H6O2, Related Products of alcohols-buliding-blocks.
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