Brun, Elodie published the artcileTotal Synthesis of (+)-Cryptocaryol A Using a Prins Cyclization/Reductive Cleavage Sequence, Synthetic Route of 57044-25-4, the publication is Journal of Organic Chemistry (2015), 80(17), 8668-8676, database is CAplus and MEDLINE.
The total synthesis of (+)-cryptocaryol A (I) was achieved in 20 steps from (R)-glycidol. The key steps were a Prins cyclization/reductive cleavage sequence to construct the C5-C11 polyol fragment, a diastereoselective aldol reaction to control the stereogenic center at C13, and a stereocontrolled reduction to introduce the stereogenic center at C15.
Journal of Organic Chemistry published new progress about 57044-25-4. 57044-25-4 belongs to alcohols-buliding-blocks, auxiliary class Epoxides,Chiral,Aliphatic hydrocarbon chain,Alcohol, name is (R)-Oxiran-2-ylmethanol, and the molecular formula is C3H6O2, Synthetic Route of 57044-25-4.
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