In 2019,Molecules included an article by Shao, Yu; Chen, Jia; Ren, Xiang-Kui; Zhang, Xinlin; Yin, Guang-Zhong; Li, Xiaopeng; Wang, Jing; Wesdemiotis, Chrys; Zhang, Wen-Bin; Yang, Shuguang; Sun, Bin; Zhu, Meifang. Safety of 3-Aminopropan-1-ol. The article was titled 《Synthesis, self-assembly and characterization of tandem triblock BPOSS-PDI-X shape amphiphiles》. The information in the text is summarized as follows:
The authors report the facile synthesis, self-assembly, and characterization of shape amphiphiles (BPOSS-PDI-X) based on isobutyl-functionalized polyhedral oligomeric silsesquioxane (BPOSS), perylene tetracarboxylic diimide (PDI), and (60)fullerene (C60) moieties. Firstly, an asym. functionalized diblock shape amphiphile precursor (BPOSS-PDI-OH) was obtained through the 1-pot reaction between perylene-3,4,9,10-tetracarboxylic dianhydride and two different amines, BPOSS-NH2 and 3-amino-1-propanol. It was further conjugated with C60-COOH to give a tri-block shape amphiphile (BPOSS-PDI-C60). Their chem. structures were thoroughly characterized by NMR, IR and MALDI-TOF MS spectrometry. To gain insights on the structure-property relation, their self-assembly in gas phase, in solution, and in solid state were characterized using traveling wave ion mobility mass spectrometry (TWIM-MS), UV/visible absorption, fluorescence emission spectrophotometer, and TEM, resp. BPOSS-PDI-OH formed more complicated dimers than BPOSS-PDI-C60. Both samples showed unique aggregation behaviors in solution with increasing concentration, which could be attributed neither to H- nor to J-type and might be related to the discrete dimers. While BPOSS-PDI-C60 could hardly crystallize into ordered structures, BPOSS-PDI-OH could form nanobelt-shaped single crystals, which may hold potential applications in microelectronics. After reading the article, we found that the author used 3-Aminopropan-1-ol(cas: 156-87-6Safety of 3-Aminopropan-1-ol)
3-Aminopropan-1-ol(cas: 156-87-6) belongs to anime.Typically the presence of an amine functional group is deduced by a combination of techniques, including mass spectrometry as well as NMR and IR spectroscopies. 1H NMR signals for amines disappear upon treatment of the sample with D2O. In their infrared spectrum primary amines exhibit two N-H bands, whereas secondary amines exhibit only one.Safety of 3-Aminopropan-1-ol
Referemce:
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts