Raman, Jayaraman Venkat et al. published their patent in 2014 |CAS: 78-26-2

The Article related to meprobamate preparation, propanediyl bischlorocarbonate preparation ammonia amidation, propanedione phosgene acylation, Aliphatic Compounds: Ureas, Carbamic Acids, Guanidines, and Their Sulfur-Containing Analogs and other aspects.Safety of 2-Methyl-2-propylpropane-1,3-diol

On February 7, 2014, Raman, Jayaraman Venkat; Sahu, Rajesh; Parikh, Ankur; Patel, Naresh published a patent.Safety of 2-Methyl-2-propylpropane-1,3-diol The title of the patent was A process for preparing highly pure meprobamate. And the patent contained the following:

The invention relates to a process for preparing highly pure meprobamate (I). Compound I was prepared by O-acylation of 2-methyl-2-propyl-1,3-propanedione with phosgene; the resulting 2-methyl-2-propyl-1,3-propanediyl bis(chlorocarbonate) underwent amidation with ammonia to give compound I. The experimental process involved the reaction of 2-Methyl-2-propylpropane-1,3-diol(cas: 78-26-2).Safety of 2-Methyl-2-propylpropane-1,3-diol

The Article related to meprobamate preparation, propanediyl bischlorocarbonate preparation ammonia amidation, propanedione phosgene acylation, Aliphatic Compounds: Ureas, Carbamic Acids, Guanidines, and Their Sulfur-Containing Analogs and other aspects.Safety of 2-Methyl-2-propylpropane-1,3-diol

Referemce:
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts