Janczewski, Lukasz’s team published research in Synthetic Communications in 2019 | 52160-51-7

Synthetic Communications published new progress about Alcohols Role: SPN (Synthetic Preparation), PREP (Preparation). 52160-51-7 belongs to class alcohols-buliding-blocks, and the molecular formula is C6H9NO, Quality Control of 52160-51-7.

Janczewski, Lukasz; Walczak, Malgorzata; Fraczyk, Justyna; Kaminski, Zbigniew J.; Kolesinska, Beata published the artcile< Microwave-assisted Cannizzaro reaction-Optimisation of reaction conditions>, Quality Control of 52160-51-7, the main research area is aldehyde microwave irradiation Cannizzaro reaction; carboxylic acid alc preparation.

The microwave-assisted Cannizzaro reaction was studied in order to develop fully reproducible synthetic protocols for transformation of aldehydes to carboxylic acid and alcs. Optimized were the following process parameters: power, temperature, and time. Aromatic, heteroaromatic and aliphatic aldehydes were used in the studies. It was found that furfural, thiophene-2-carbaldehyde, pyridinecarboxaldehyde and aromatic aldehydes react under mild conditions, while 1-methyl-pyrrole-2-carboxaldehyde derivatives and aliphatic aldehydes require more drastic reaction conditions and a longer exposure time to microwave radiation.

Synthetic Communications published new progress about Alcohols Role: SPN (Synthetic Preparation), PREP (Preparation). 52160-51-7 belongs to class alcohols-buliding-blocks, and the molecular formula is C6H9NO, Quality Control of 52160-51-7.

Referemce:
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts