Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 13651-14-4, name is (2,3-Dimethylphenyl)methanol. This compound has unique chemical properties. The synthetic route is as follows. Application In Synthesis of (2,3-Dimethylphenyl)methanol
In a fixed-bed reactor having an inner diameter of 10 mm, 1 g of the Cu5wt%-Pd4wt%-K5wt%/Al203 catalyst prepared in Example 1 was charged in a constant temperature zone of the reaction tube, and both ends were filled with quartz sand and quartz wool to ensure the reaction. The airflow was stable and evenly distributed. The sealing device was reductively activated with hydrogen (25 ml/min) at 350 C for 7 hours. Then change the carrier gas to argon and the argon flow was adjusted to 200ml/h and pressure to 3.5MPa. Then the temperature was adjusted to 150C; The reaction was started by continuously feeding o-nitroaniline:fatty alcohol:distilled water according to a mass ratio of 1:12:10 with a high pressure pump. The feed flow of o-nitroaniline, fatty alcohol, and distilled water was 0.7 g/liter/h. After the reaction product was cooled by the condenser and then entered the gas-liquid separator, the liquid product was collected. The results of the experiments with different fatty alcohols are shown in Table 2.
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Reference:
Patent; Zhejiang University of Technology; Zhang Qunfeng; Cheng Zheng; Feng Feng; Xu Xiaoliang; Ma Lei; Lu Chunshan; Li Xiaonian; (12 pag.)CN105037274; (2018); B;,
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