Brief introduction of

Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps,and cheap raw materials. 261763-21-7, name is (5-Chloro-2-(trifluoromethyl)phenyl)methanol. A new synthetic method of this compound is introduced below., Product Details of 261763-21-7

Dissolve (5-chloro-2-trifluoromethylphenyl)-methanol (347 mg, 1.66 mmol) in dichloromethane (10 mL). Add pyridinium chlorochromate (717 mg, 3.32 mmol) and stir for 2 h. Dilute with diethyl ether and stir for 1 h. Filter and concentrate. Chromatograph on silica gel eluting with 10% ethyl acetate in hexane to give the title compound as a clear EPO oil (285 mg, 82%). 1HNMR (400 MHz, MeOH-d4) delta 10.33 (s, IH), 7.90 (s, IH), 7.69 (d, IH5 J = 8.4 Hz), 7.54 (d, IH, J = 8.4 Hz).

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Reference:
Patent; ELI LILLY AND COMPANY; WO2006/44454; (2006); A1;,
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