Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 79944-63-1, name is (3-Amino-5-chlorophenyl)methanol. This compound has unique chemical properties. The synthetic route is as follows. Recommanded Product: 79944-63-1
Example A24; a) Preparation of intermediate 83; [Show Image] 3-Amino-5-chloro-benzenemethanol (0.0194 mol) was added in one portion to a solution of intermediate 77 (0.0162 mol) in 1,4-dioxane (80 ml). DIPEA (0.0194 mol) was added. The resultant reaction mixture was stirred for 8 hours at room temperature. CH2Cl2 (50 ml) and brine (50 ml) were added. The layers were separated. The organic layer was washed with brine (2 x 20 ml). The organic layers were combined, dried (MgSO4), filtered and the solvent was evaporated, yielding 6 g (90%) of intermediate 83.
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Reference:
Patent; Janssen Pharmaceutica NV; EP1904461; (2008); A2;,
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