Application of 624-08-8, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 624-08-8, name is Heptadecan-9-ol, molecular formula is C17H36O, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
From 0 C in a round flask was added the p- toluenesulfonyl chloride (5.5g) and the mixture was stirred and then placed in methylene chloride (150mL). Put Then, hepta-decane-9-ol followed by the addition of (5g) and slowly diluted in methylene chloride (5mL), triethylamine (7mL) and triethylamine hydrochloride (3.71g), and the mixture was stirred for 90 minutes . MC and the organic layer with brineAnd then extracted to remove the remaining water over anhydrous magnesium sulfate, and after evaporation of the solvent was recrystallized from a MC and MeOH to give the Heptadecane-9-yl 4-methlybenzenesulfornate (compound f-4) as a white solid (yield: 64% ).
While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 624-08-8, Heptadecan-9-ol.
Reference:
Patent; Pusan National University Industry-Academic Cooperation Foundation; Hwang, Do Hun; Kim, Ji Hun; Kim, Hee Woon; Im, Jong Min; (52 pag.)KR101495152; (2015); B1;,
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