29-Sep News New downstream synthetic route of 56-81-5

According to the analysis of related databases, 624-95-3, the application of this compound in the production field has become more and more popular.

Related Products of 624-95-3, Adding some certain compound to certain chemical reactions, such as: 624-95-3, name is 3,3-Dimethylbutan-1-ol,molecular formula is C6H14O, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 624-95-3.

12.2 g of 3, 3-Dimethyl-l-butanol of 98% purity (117.3 mmol) and 0.049 g 4- Acetamido-TEMPO (0. 223MMOL) are charged in a jacketed glass reaction flask as in Example I. Sodium borate (0.294 g, 0.76 mmol), NAHC03 (1. 472 g, 17. 5MMOL) and NACL (2 g) are dissolved in water (25 cc) and the aqueous solution is added to the stirred organic fraction at 1000RPM in the reaction flask. The stirred suspension is cooled to 0C and the emulsion is re-adjusted to pH 8.6 using 40% solution OF NAOH. When the temperature of the reactants reached 0C, 69.8 g (123.1 mmol) of 13.1% aqueous NAOCI solution are pumped in via a gas-tight syringe over 55 minutes. The reaction mixture is stirred for an additional 15 min at 0C and the organic layer is sampled for GC assay. The yield of 3, 3-dimethylbutyraldehyde is 88.3% at 2 MIN of post bleach-addition time and 92. 1 % at 15 min reaction time.

According to the analysis of related databases, 624-95-3, the application of this compound in the production field has become more and more popular.

Reference:
Patent; THE NUTRASWEET COMPANY; WO2004/67484; (2004); A2;,
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