Adding a certain compound to certain chemical reactions, such as: 7397-62-8, Butyl 2-hydroxyacetate, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, SDS of cas: 7397-62-8, blongs to alcohols-buliding-blocks compound. SDS of cas: 7397-62-8
47.6 g (0.5 mol) of phenol, 134.2 g (1.04 mol) of butyl hydroxyacetate, and 0.36 g of catalyst Mo2P5-MCM-48 (molar ratio of Mo1P3 and MCM-48: 25:100) were mixed and stirred, and the temperature was raised to 100-120 C, the rectification water was reacted for 2 hours in this process. When the top of the column is substantially anhydrous, the reaction is completed, the temperature is lowered to room temperature, the catalyst is removed by suction filtration, the catalyst is continuously activated after the catalyst is activated, the obtained mother liquid is distilled to recover the solvent, and then the unsubstituted butyl hydroxyacetate and phenol are separated by distillation to obtain the product benzene. Butyl oxyacetate 69.6 g, purity 98.2%, selectivity 99.2%, yield 65.78%. The prepared butyl phenoxyacetate was detected by nuclear magnetic resonance, and the nuclear magnetic resonance spectrum was as shown in Fig. 2.
At the same time, in my other blogs, there are other synthetic methods of this type of compound,7397-62-8, Butyl 2-hydroxyacetate, and friends who are interested can also refer to it.
Reference:
Patent; Shandong Runbo Biological Technology Co., Ltd.; Sun Guoqing; Hou Yongsheng; Chi Zhilong; He Enjing; Hu Yishan; (8 pag.)CN108947841; (2018); A;,
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