Synthetic Route of 56-81-5, Adding some certain compound to certain chemical reactions, such as: 56-81-5, name is Propane-1,2,3-triol,molecular formula is C3H8O3, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 56-81-5.
General procedure: In(OTf)3 (5.6 mg, 10 mumol, 1 mol %) was added to a mixture of cyclohexanone dimethylacetal (144 mg, 1.00 mmol) and finely ground 2,2-dimethyl-1,3-propanediol (111 mg, 1.10 mmol) and the reaction mixture stirred at room temperature for 30 min. At this time, residual MeOH was removed under reduced pressure and the crude residue passed through a short plug of basic alumina, which was washed with hexane (2×2 mL). The solvent was removed under reduced pressure to give the product, as a colourless oil (170 mg, 92%).
According to the analysis of related databases, 56-81-5, the application of this compound in the production field has become more and more popular.
Reference:
Article; Smith, Brendan M.; Kubczyk, Tomasz M.; Graham, Andrew E.; Tetrahedron; vol. 68; 38; (2012); p. 7775 – 7781;,
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