Application of 6006-82-2, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 6006-82-2, name is 2-(Benzo[d][1,3]dioxol-5-yl)ethanol, molecular formula is C9H10O3, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
B. 1-acetoxy-2-[(3,4-methylenedioxy)phenyl]ethane To a stirred solution of 2-(3,4-methylenedioxy)phenyl-1-ethanol (1.68 g, 10 mmol) in dry pyridine was added acetic anhydride and the resultant reaction mixture was stirred at 80 C. for 1 h. The reaction mixture was poured into ice-water and was extracted with ether (2*75 ml). The combined ether extract was washed with water (2*50 ml), 5% HCl (2*50 ml) and then with 5% NaHCO3 (2*50 ml). The organic layer was dried over magnesium sulfate and the solvent was removed under reduced pressure to give 1-acetoxy-2-[(3,4-methylenedioxy)phenyl]ethane as a solid (1.7 g, 81% yield).
According to the analysis of related databases, 6006-82-2, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Texas Biotechnology Corporation; US6432994; (2002); B1;,
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