Electric Literature of 34626-51-2, With the rapid development and complex challenges of chemical substances, the synthesis of new drugs is usually one of the most effective ways to increase yield.34626-51-2, name is 5-Bromopentan-1-ol, molecular formula is C5H11BrO, molecular weight is 167.0442, as common compound, the synthetic route is as follows.
5-bromopentanol (8 g) was dissolved in DICHLOROMETHANE (100 mL) and was chilled in an ice bath. Dihydropyran (9 g) was added dropwise followed by P-TOLUENE SULFONIC acid monohydrate (1 g). The mixture was allowed to slowly warm to room temperature and stirred for 18 HOURS. The mixture was diluted with 200 mL ether, washed with 10% INA (: H (100 mL) and dried over MgSO4 to give the title compound. DZ (CDC13, 62.9 MHz): 19.7, 25.0, 25.5, 28. 9,30. 7,32. 6,33. 7,62. 4,67. 2 and 89. 9.
Statistics shows that 34626-51-2 is playing an increasingly important role. we look forward to future research findings about 5-Bromopentan-1-ol.
Reference:
Patent; THE UNIVERSITY COURT OF THE UNIVERSITY OF ABERDEEN; WO2004/98582; (2004); A2;,
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