Reference of 124-68-5, Adding some certain compound to certain chemical reactions, such as: 124-68-5, name is 2-Amino-2-methyl-1-propanol,molecular formula is C4H11NO, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 124-68-5.
To a stirred solution of 2-amino-2-methylpropan-1-ol (3.0 g, 33.65 mmol) in DCM (200 ml) was added aqueous NaHCO3 (8.4 g, 100.95 mmol in 100 ml water) at 0C and 50% wt20 CbzClintoluene (11.4 g, 33.65 mmol) was added drop wise over 15mm After the addition,the reaction mixture was warmed to RT and stirred for 16 h. The reaction mixture was diluted with DCM and organic layer was dried over Na2504, concentrated under reduced pressure. The product was purified by flash column using 20% ethyl acetate in pet ether as eluent to afford 4.2 g of colorless oil. LC-MS (ES+) [M+1]: 224.2
According to the analysis of related databases, 124-68-5, the application of this compound in the production field has become more and more popular.
Reference:
Patent; ORION CORPORATION; WANG, Shouming; KUMPULAINEN, Esa; PYSTYNEN, Jarmo; POHJAKALLIO, Antti; HAIKARAINEN, Anssi; (92 pag.)WO2016/193551; (2016); A1;,
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