Reference of 13826-35-2, Adding some certain compound to certain chemical reactions, such as: 13826-35-2, name is (3-Phenoxyphenyl)methanol,molecular formula is C13H12O2, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 13826-35-2.
To a solution of triphenyl phosphine (4.52 g; 17.2 mmol) and 3-phenoxybenzyl alcohol (3.44 g; 17.2 mmol) in THF (20 mL) kept in an ice bath was added a solution of 1a (4.61 g; 17.2 mmol) and diisopropyl azodicarboxylate (95%, 3.66 g; 17.2 mmol) in THF (20 mL). The reaction mixture was stirred at 0 C for 2 h and monitored by TLC. The solvent was removed on the rotary evaporator, leaving a yellow oil which was purified by flash chromatography (silica gel/ethyl acetate/hexane) to yield a white solid (6.33 g; 82% yield), mp 75-77 C. 1H NMR (CDCl3): delta 1.49 (s, 9H), 3.65 (d, 2H), 3.72 (s, 3H), 4.79 (s, 2H), 4.77 (t, J = 13.6 Hz, 1H), 6.90-7.03 (m, 4H), 7.10 (d, 2H), 7.30-7.39 (m, 3H).
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 13826-35-2, (3-Phenoxyphenyl)methanol, other downstream synthetic routes, hurry up and to see.
Reference:
Article; Dou, Dengfeng; Tiew, Kok-Chuan; Mandadapu, Sivakoteswara Rao; Gunnam, Mallikarjuna Reddy; Alliston, Kevin R.; Kim, Yunjeong; Chang, Kyeong-Ok; Groutas, William C.; Bioorganic and Medicinal Chemistry; vol. 20; 6; (2012); p. 2111 – 2118;,
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