Synthetic Route of 7073-69-0, Adding some certain compound to certain chemical reactions, such as: 7073-69-0, name is 2-(2-Bromophenyl)propan-2-ol,molecular formula is C9H11BrO, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 7073-69-0.
Under a nitrogen stream, 3-(3-chloro-2-iodophenyl)-6,9-diphenyl-9H-carbazole (89.6 g,161.2 mmol) and 2-(2-bromophenyl)propan-2-ol (41.6 g, 193.4 mmol), Pd2(dba)3 (7.4 g, 8.1 mmol), PPh3 (8.5 g, 32.2 mmol), Cs2CO3 (126.0 g,386.9 mmol), toluene (1000 ml) were mixed and stirred at 120 C for 16 hours. After the reaction was completed, the reaction mixture was extracted with methylenechloride, added with MgSO4 and filtered. The solvent was removed from the obtained organic layer, and the residue was purified by column chromatography (Hexane: EA =6: 1 (v / v)) to obtain 1-chloro-7,10-diphenyl-7H-phenanthro[9,10-c]carbazole (37.4 g, yield 46%).
According to the analysis of related databases, 7073-69-0, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Doosan Co., Ltd; Cho Hyeon-jong; Um Min-sik; Kim Tae-hyeong; Han Song-i; (65 pag.)KR2018/71880; (2018); A;,
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