Adding a certain compound to certain chemical reactions, such as: 2173-69-5, 2-Methyl-2-phenyl-1-propanol, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound, HPLC of Formula: C10H14O, blongs to alcohols-buliding-blocks compound. HPLC of Formula: C10H14O
2-methyl-2-phenyl-propanol (Intermediate 3) (0.5 kg) and pyridine (268 ml) were charged to a reactor and chilled to 0C. Acetic anhydride (680 gms) was slowly added through a dropper at 10-20C. The mixture was stirred for 2 hours at 10-20C. Ethyl acetate (1.5 ltr) was added and chilled water (2 ltrs) was slowly added through a dropper at 10-20C. The mixture was stirred FOR 4 hr. The ethyl acetate layer was separated and 10% chilled dilute HC1 was added. The ethyl acetate layer was then washed with sodium bicarbonate until a pH of 7 was obtained. The ethyl acetate layer was dried with sodium sulphate and concentrated under vacuum. The resulting oil was distilled under vacuum (15 mm OF HG). at 80-100C.
The synthetic route of 2173-69-5 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; CIPLA LIMITED; WAIN, Christopher, Paul; WO2005/19175; (2005); A1;,
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