Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps,and cheap raw materials. 10160-28-8, name is Non-8-yn-1-ol. A new synthetic method of this compound is introduced below., Computed Properties of C9H16O
Example 2Part A: Synthesis of Pentadeca-8,10-diyn-l-olTo a stirred solution of 1-iodo-hex-l-yne (6.2 g, 29.80 mmol) and non-8-yn-l-ol (2.46 g, 17.53 mmol) in pyrrolidine (50 ml) under an argon atmosphere, was added copper(I) iodide (2.98 mmol, 0.57 g). After stirring at room temperature for 30 min, the mixture was hydrolysed with a saturated aqueous solution of ammonium chloride and extracted with diethyl ether. The organic extract was dried over MgSO4 and the solvent was removed in vacuo. Column chromatography (SiO2, EtOAc-hexane: 2:1) gave 3.35 g (15.19 mmol, 87 %) of pure pentadeca-8,10-diyn-l-ol. 1H-NMR (CDCl3, 400 MHz): delta[ppm] = 0.89 (3H, t, J = 7.3 Hz)5 1.26 – 1.62 (14H, m), 2.24 (4H, t, J = 6.6 Hz), 3.62 (2H, t, J = 7.0 Hz)
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Reference:
Patent; COMMONWEALTH SCIENTIFIC AND INDUSTRIAL RESEARCH ORGANISATION; WO2008/31157; (2008); A1;,
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