Electric Literature of 1805-32-9, Adding some certain compound to certain chemical reactions, such as: 1805-32-9, name is 3,4-Dichlorobenzyl alcohol,molecular formula is C7H6Cl2O, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 1805-32-9.
Under nitrogen, 4-aminobenzenesulfonamide (172 mg, 1 mmol), [Cp * IrCl2] 2 (8 mg, 0.01 mmol,1 mol%), cesium carbonate (65 mg, 0.2 mmol), 3,4-dichlorobenzyl alcohol (212 mg, 1.2 mmol)The alcohol (1.0 mL) was added sequentially to a 25 mL Schlenk reaction flask. The mixture was reacted at 120 C for 12 hoursAfter cooling to room temperature, the solvent was removed under vacuum. And then purified by column chromatography (developing solvent: ethyl acetate / n-hexane)The pure title compound was obtained in a yield of 92%
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 1805-32-9, 3,4-Dichlorobenzyl alcohol, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; NANJING UNIVERSITY OF SCIENCE AND TECHNOLOGY; LI, FENG; LU, LEI; MA, JUAN; (16 pag.)CN106146358; (2016); A;,
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