Electric Literature of 7287-81-2, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 7287-81-2, name is 1-(m-Tolyl)ethanol, molecular formula is C9H12O, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
Take a reaction tube, add 49 mg of sodium azide, 41 mg of 1-(3-methylphenyl)ethanol, and 400 uL of trifluoroacetic acid.200 uL of methanesulfonic acid and 1.0 mL of n-hexane were stirred at 40 C for 6 hours.After the reaction was quenched with 10mL of sodium hydroxide solution was added, extracted 3 times with ethyl acetate, the organic was washed with brine by adding 5mL, the combined organic phases,The nuclear magnetic yield of m-methylaniline was 53%.
While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 7287-81-2, 1-(m-Tolyl)ethanol.
Reference:
Patent; Peking University; Jiao Ning; Liu Jianzhong; (27 pag.)CN109134267; (2019); A;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts