Electric Literature of 702-98-7, Adding some certain compound to certain chemical reactions, such as: 702-98-7, name is 2-Methyladamantan-2-ol,molecular formula is C11H18O, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 702-98-7.
To a stirred mixture of 2-methyl-2-adamantanol 14 (200 mg, 1.21 mmol), triethylamine(243 mg, 2.41 mmol) and acetic anhydride (246 mg, 2.41 mmol), 4-dimethylaminopyridine (DMAP) (18 mg, 0.12 mmol) was added as the acetylation catalyst. The mixture was stirred at room temperature for 72 h (TLC minitoring,hexane/ether 3:1). Petroleum ether was added and the mixture was washed withHCl 5%, saturated NaHCO3, brine and dried (Na2SO4). After solvent evaporation the residue was chromatographed on silica gel column using hexane-ether 4:1 as eluent to afford 150 mg (60 %) of pure acetyl derivative 20 (a second fraction including 2-methylene adamantane was obtained).
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 702-98-7, 2-Methyladamantan-2-ol, other downstream synthetic routes, hurry up and to see.
Reference:
Article; Kolocouris, Antonios; Koch, Andreas; Kleinpeter, Erich; Stylianakis, Ioannis; Tetrahedron; vol. 71; 16; (2015); p. 2463 – 2481;,
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