With the rapid development and complex challenges of chemical substances, the synthesis of new drugs is usually one of the most effective ways to increase yield.1777-82-8, name is (2,4-Dichlorophenyl)methanol, molecular formula is C7H6Cl2O, molecular weight is 177.03, as common compound, the synthetic route is as follows.Product Details of 1777-82-8
General procedure: In a 50ml Pyrex round-bottom flask, a mixture of alcohol (1mmol), TBATB (10-20mg, 0.02-0.04mmol) in 10ml of CH3CN was exposed to blue or violet light LED irradiation at room temperature under an air atmosphere with stirring. The progress of the photocatalytic oxidation reaction was monitored by TLC on silica gel plates. The reaction mixture externally irradiated until the alcohol was completely consumed.
At the same time, in my other blogs, there are other synthetic methods of this type of compound,1777-82-8, (2,4-Dichlorophenyl)methanol, and friends who are interested can also refer to it.
Reference:
Article; Mardani, Atefeh; Heshami, Marouf; Shariati, Yadollah; Kazemi, Foad; Abdollahi Kakroudi, Mazaher; Kaboudin, Babak; Journal of Photochemistry and Photobiology A: Chemistry; vol. 389; (2020);,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts