Synthetic Route of 647-42-7, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 647-42-7, name is 3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctan-1-ol. This compound has unique chemical properties. The synthetic route is as follows.
C6F13-CH2CH2-O-CH2CH=CH2197.11g (488mmol) was dropped in 2 hours. It agitated at 110 degrees C after the end of dropping for 2 hours. Then, it lowered to 70 degrees C. NaOH solution 25.07g was added 0.1%, and it stirred for 2 hours. drying in 60 degrees C / 5KPa — after the end of drying, and the temperature — cull — bora — fin 3(made in Japanese Emba Illo Kem Carzou)2.51g was added, and it stirred for 2 hours. It filtered with the 0.1micrometer PTFE membrane filter, steam distillation of the filtrate was carried out using 100 degrees C / 5KPa, and the water 62.5g, and 206.3 g of object compounds (compound B1) were obtained (89% of yield).
According to the analysis of related databases, 647-42-7, the application of this compound in the production field has become more and more popular.
Reference:
Patent; KAO CORPORATION; WATARAI, ETSUKO; IGARASHI, TAKANORI; YAGO, YUKO; UEHARA, KOICHI; (20 pag.)JP2017/25048; (2017); A;,
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