Electric Literature of 14320-38-8, Adding some certain compound to certain chemical reactions, such as: 14320-38-8, name is Cyclopent-3-enol,molecular formula is C5H8O, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 14320-38-8.
Step 1: Toluene-4-sulfonic acid cyclopent-3-enyl ester Cyclopent-3-ene-1-ol (200 mg, 2.38 mmol) was dissolved in pyridine (2.5 ml) and p-toluenesulfonyl chloride (558 mg, 2.92 mmol) was added portionwise at 0 C. After the addition was completed the reaction mixture was stirred at 0 C. for 3 h and then kept in the fridge overnight. Then it was poured into to a mixture of ice and diluted HCl (pH ~5). The solid was filtered off, washed with diluted HCl and dried to obtain the title compound as off-white solid (447 mg, 79%). MS (EI): 256.2 (M+NH4)+.
According to the analysis of related databases, 14320-38-8, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Banner, David; Ceccarelli, Simona M.; Grether, Uwe; Haap, Wolfgang; Hilpert, Hans; Kuehne, Holger; Mauser, Harald; Plancher, Jean-Marc; Sanchez, Ruben Alvarez; US2010/317647; (2010); A1;,
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