Synthetic Route of 41175-50-2, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situation. 41175-50-2, name is 1,2,3,5,6,7-Hexahydropyrido[3,2,1-ij]quinolin-8-ol, molecular formula is C12H15NO, The compound is widely used in many fields, so it is necessary to find a new synthetic route. The downstream synthesis method of this compound is introduced below.
To a 150 mL round bottom flask was added 40 mL of toluene, followed by the addition of 18.9 g (0.1 mol) of compound 3, phthalic anhydride14.8 g (0.1 mol), stirred and stirred. The mixture was refluxed for 5 hours to gradually form a solid. The solid was removed by suction filtration and recrystallized from methanol to give Dark red solid.
According to the analysis of related databases, 41175-50-2, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Xuchang University; Hou Xufeng; Xu Zhihong; Li Bolun; Zhan Qiangqiang; Cheng Zijie; (23 pag.)CN107090191; (2017); A;,
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