The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 702-23-8, name is 2-(4-Methoxyphenyl)ethanol. This compound has unique chemical properties. The synthetic route is as follows. Recommanded Product: 2-(4-Methoxyphenyl)ethanol
6 (2.0 g, 13.1 mmol) was dissolved in dry toluene (50mL), dry CaCO3 (3.94 g, 39.4 mmol), PCl5 (5.47 g, 26.3 mmol) were added slowly over a period of 40 min under argon atmosphere at 0 C; temperature in the mixture was allowed to reach RT and stirred for another 3 h. The mixture was poured into ice-cold saturated NaHCO3 solution (20 mL) and extracted twice with diethyl ether (100 mL). The organic layer was dried with Na2SO4 and evaporated. Purification by silica gel column chromatography (n-hexane-ethyl acetate 9:1 (v/v)) yielded a yellow oil:7 (1.95 g, 87 %).
With the rapid development of chemical substances, we look forward to future research findings about 702-23-8.
Reference:
Article; Blaess, Markus; Bibak, Nelly; Claus, Ralf A.; Kohl, Matthias; Bonaterra, Gabriel A.; Kinscherf, Ralf; Laufer, Stefan; Deigner, Hans-Peter; European Journal of Medicinal Chemistry; vol. 153; (2018); p. 73 – 104;,
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