Reference of 7541-49-3 ,Some common heterocyclic compound, 7541-49-3, molecular formula is C20H40O, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc., below Introduce a new synthetic route.
Platinum oxide (PtO2, 1.15 g, 6.61 mmol) is added to a solution of phytol (30.00 g, 101.20 mmol) in THF (450 mL) under argon and the medium is placed under 1 bar of dihydrogen, then stirred for 4 hours at room temperature. After filtration through celite rinsed with THF, a black oil of molecule A27 is obtained after concentration under reduced pressure. Yield: 29.00 g (96%)1H-NMR (CDCl3, ppm): 0.84 (6H); 0.86 (6H); 0.89 (3H); 1.00-1.46 (22H); 1.46-1.68 (3H); 3.61-3.73 (2H).
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 7541-49-3, 3,7,11,15-Tetramethylhexadec-2-en-1-ol, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; ADOCIA; GEISSLER, Alexandre; (119 pag.)US2019/275108; (2019); A1;,
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