Synthetic Route of 534-03-2, Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps,and cheap raw materials. 534-03-2, name is 2-Aminopropane-1,3-diol. A new synthetic method of this compound is introduced below.
Add 735ml of ethyl acetate in the flask cooled to 0C under a stream of nitrogen, Sulforhodamine B acid chloride 85g (147mmol) added to the agitation. And serinol 16.1g (177mmol), N, N-dimethylaminopyridine 0.899g (7.37mmol), triethylamine and 38.3g (53ml, 295mmol) was further added the mixture was stirred at room temperature for 15 hours.Then the solid was obtained 70.1.5g compound (yield 69%) of the title mixture of the red solid obtained by concentration under reduced pressure by a rotary evaporator by the formula 6-4 to by washing with ethyl acetate.
These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,534-03-2, its application will become more common.
Reference:
Patent; Cheil Industries Co.Ltd; Kim, Won Jung; Kang, Gyung Hee; Park, Chae Won; Sin, Myung Yeop; Jeon, Hwan Sung; Jung, Uii Soo; Hwang, Gi Wook; (40 pag.)KR2015/89702; (2015); A;,
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