Application of 27129-87-9, Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps,and cheap raw materials. 27129-87-9, name is (3,5-Dimethylphenyl)methanol. A new synthetic method of this compound is introduced below.
The 0.91 g (0.0067 muM) of 3, 5 – dimethyl benzoic alcohol and 0.4 g of the dispersed GO – Ti 10 ml in tetrahydrofuran, and in the oil bath heated to 70 C, 1 . 89 g (0.0167 muM) of 30 wt % aqueous hydrogen peroxide solution in tetrahydrofuran is slowly added, keeping the temperature reaction 5 h, by HPLC detection, 3, 5 – dimethylphenyl methanol conversion rate is 91.3%, 3, 5 – dimethyl formaldehyde selectivity of 98.2%. After filtering to remove the catalyst concentrated filtrate, separation by silica gel column chromatography to obtain 3, 5 – dimethyl benzaldehyde 0.85 g, yield: 94.5%.
These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,27129-87-9, its application will become more common.
Reference:
Patent; Shenyang Pharmaceutical University; Wang Qinghe; Cheng Maosheng; Ma Wenxi; Tong Qiaolin; Wang Shicheng; (8 pag.)CN108395369; (2018); A;,
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