The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 16700-55-3, name is (2,6-Dimethoxyphenyl)methanol. This compound has unique chemical properties. The synthetic route is as follows. Quality Control of (2,6-Dimethoxyphenyl)methanol
To 15 ml of dichloromethane were added 1.1 g of 3-[bis(4-fluorophenyl)methyl]-4-piperidinone hydrochloride, 1.7 ml of isopropyl ethylamine and 0.6 g of 2, 6-dimethoxybenzyl alcohol and the mixture was stirred at room temperature.. Then, 0.8 ml of EPPA was added thereto and the mixture was allowed to stand at room temperature for 4 days.. The solvent was distilled off under reduced pressure, and the residue was purified by subjecting it to silica gel column chromatography (40 g, ethyl acetate: hexane = 1: 1) to obtain 0.88 g of the title compound (yield: 60%). mp 125-126C. IR (KBr).. 1705, 1595, 1505, 1470, 1250, 1215, 1110, 830, 555, 525 cm-1.
With the rapid development of chemical substances, we look forward to future research findings about 16700-55-3.
Reference:
Patent; Takeda Chemical Industries, Ltd.; EP1460062; (2004); A1;,
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