Reference of 116-02-9, Adding some certain compound to certain chemical reactions, such as: 116-02-9, name is 3,3,5-Trimethylcyclohexanol,molecular formula is C9H18O, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 116-02-9.
a) 426g (3,00 Mol) of Homomenthol is added to the above-mentioned filtrate, the temperature is raised to 60C and under stirring and a vacuum of 100mbar the Ethyl acetate is distilled off the reaction mixture. Then 56g of Sulfuric acid are added at a temperature of 50C within 20minutes, stirring is continued for 6h. For work-up 500g of Toluene are added to the reaction mixture and after cooling to 5-10C the dosage of 500g of iced water follows. After separation of the water layer the organic layer is washed to neutral with aqueous Sodium hydroxide solution (10% w/w) and finally with saturated aqueous Sodium chloride solution. After separation of the water layer the organic layer is distilled resulting 250g (0,93 Mol) of product. Yield (overall): 58% of theory.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles. 116-02-9, 3,3,5-Trimethylcyclohexanol, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; Symrise AG; Stuhlmann, Dominik; Meyer, Imke; Koch, Oskar; Oertling, Heiko; Herrmann, Martina; Goemann, Claudia; EP2810934; (2014); A1;,
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