Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 20712-12-3, name is (2-Amino-5-bromophenyl)methanol. This compound has unique chemical properties. The synthetic route is as follows. COA of Formula: C7H8BrNO
General procedure: A mixture of 2-aminobenzyl alcohol 1 (0.2 mmol), allylic alcohol 2(0.4 mmol), [IrCp*Cl2]2 (0.0020 mmol, 1.0 molpercent), and KOH (0.2 mmol) were dissolved in anhyd toluene (1 mL) in a 25-mL Schlenk tube. The system was flushed with N2 and allowed to react at the specified temperatureand for the specified time. The mixture was allowed to cool to r.t. and filtered through a short silica gel column (washed with EtOAc). Removal of the solvent left an oil that was separated by column chromatography (silica gel, EtOAc?hexane) to give the quinoline.
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Reference:
Article; Chen, Shu-Jie; Lu, Guo-Ping; Cai, Chun; Synthesis; vol. 47; 7; (2015); p. 976 – 984;,
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