Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 7541-49-3, name is 3,7,11,15-Tetramethylhexadec-2-en-1-ol. This compound has unique chemical properties. The synthetic route is as follows. COA of Formula: C20H40O
Example 75Synthesis of 1-O-(3,7,11,15-tetramethylhexadec-2-enyl)-D-glucoside 3.4 g (8.7 mmol) of 13-D-Glucose pentaacetate and 2.0 g (6.7 mmol) of phytol were dissolved in dry acetonitrile (7 mL). 1.70 mL (13.4 mmol) of boron trifluoride diethyl etherate complex was added to the solution with cooling on ice. The reaction mixture was allowed to warm up slowly to room temperature while being stirred for 18 hours before addition of 2.8 mL (20 mmol) of triethylamine at 0 C. The resulting solution was diluted with ethyl acetate, and washed with water, 1M hydrochloric acid, saturated sodium bicarbonate aqueous solution, and saturated brine, successively, and dried over sodium sulfate. After filtration, the filtrate was concentrated to obtain a crude product of 1-O-(3,7,11,15-tetramethylhexadec-2-enyl)-D-glucopyranoside tetraacetate.
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Reference:
Patent; Chemgenesis Incorporated; US2012/264923; (2012); A1;,
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