Introduction of a new synthetic route about 13807-89-1

While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 13807-89-1, 2-((4-Methoxybenzyl)oxy)ethanol.

Application of 13807-89-1, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 13807-89-1, name is 2-((4-Methoxybenzyl)oxy)ethanol. This compound has unique chemical properties. The synthetic route is as follows.

Methanesulfonic acid 2-(4-methoxybenzyloxy) ethyl ester A solution of 2-(4-methoxybenzyloxy)ethanol (Intermediate 18) (2.26g, 12.4mmol) and diisopropylethylamine (6.7ml, 37.2mmol) in 15mL dry DCM, cooled to O0C under a nitrogen atmosphere, was treated dropwise with a solution of methanesulfonyl chloride (1.5ml_, 18.6mmol) in 1OmL DCM. The reaction mixture was stirred at RT for 16h, then water was added. The organic layer was separated, dried (MgSO4) and concentrated. Purification by chromatography (Redisep cartridge) eluting with ethyl acetate/cyclohexane afforded the title compound as an oil. Yield: 2.5g (77%) LC-MS (Method 4): Rt 2.81 mins, molecular ion not observed

While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 13807-89-1, 2-((4-Methoxybenzyl)oxy)ethanol.

Reference:
Patent; ARGENTA DISCOVERY LTD.; WO2008/96093; (2008); A1;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts