Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps,and cheap raw materials. 16545-68-9, name is Cyclopropanol. A new synthetic method of this compound is introduced below., Formula: C3H6O
Water (300 ml),Cyclopropanol (500 ml),N, N-diethyl-2,3,3,3-tetrafluoropropanamide (900 g, 4.47 mol),98% sulfuric acid (600 ml) was placed in the reaction flask,The temperature was raised to 130 C and refluxed for 12 hours.Reaction completed,Atmospheric distillation,Fractions of around 127 C were collected to give cyclopropyl 2,3,3,3-tetrafluoropropionate,The yield was 90%Purity 98.6%.
If you are interested in these compounds, you can also browse my other articles.Thank you for taking the time to read this article. I hope you enjoyed it, 16545-68-9, Cyclopropanol.
Reference:
Patent; Zhao, Manliang; (9 pag.)CN106278887; (2017); A;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts