Reference of 764-48-7 ,Some common heterocyclic compound, 764-48-7, molecular formula is C4H8O2, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc., below Introduce a new synthetic route.
To a round bottom flask 1 L, 1,1′-thiocarbonyldiimidazole 3.6 g (20.2 mmol), 2-hydroxyethyl vinyl ether (95% purity) 1.9 mL (20.2 mmol) and toluene 60mL was added, 60 at was refluxed for 6 hours. Then allowed to cool to room temperature, potassium hydroxide 0.05g (0.89mmol) and benzyl mercaptan 2.4mL of (20.5 mmol) was added, and the mixture was refluxed for 6 hours again 60 C.
These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route,764-48-7, its application will become more common.
Reference:
Patent; UNIVERSITYOF FUKUI; MARUZENPETROCHEMICAL COMPANY LIMITED; SUGIHARA, SHINJI; (22 pag.)JP5818142; (2015); B2;,
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