The origin of a common compound about 355-80-6

While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 355-80-6, 2,2,3,3,4,4,5,5-Octafluoro-1-pentanol.

Application of 355-80-6, The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 355-80-6, name is 2,2,3,3,4,4,5,5-Octafluoro-1-pentanol. This compound has unique chemical properties. The synthetic route is as follows.

Synthesis of 4-methyl-2-[(2,2,3,3,4,4,5,5-octafluoropentyl)oxy]-1,3,2-dioxaphosphinane 29.90g (0.129mol) of 2,2,3,3,4,4,5,5-octafluoro-1-pentanol and 15.65g (0.155mol) of triethylamine were dissolved in 180ml of hexane to prepare a solution, and another solution was prepared by dissolving 20.00g (0.129mol) of 2-chloro-4-methyl-1,3,2-dioxaphosphinane in 20ml of hexane. The latter solution was dropped to the former solution while the former solution was fervently agitated at -10C for 3.5 hours. During the process, a formation of a white triethylammonium hydrochloride precipitate was to be found. The reaction mixture was further agitated for 3 hours at room temperature and allowed to stand for one night. The triethylammonium hydrochloride was separated from the resulting mixture and washed with hexane. Then, hexane was removed under the atmospheric pressure, and the residues were distilled under vacuum, obtaining 32.53g of a compound which is 4-methyl-2-[(2,2,3,3,4,4,5,5-octafluoropentyl)oxy]-1,3,2-dioxaphosphinane, represented by the following Chemical Formula 1A, The yield was 72%.

While traditionally a conservative industry, chemical producers will need to modernize their PR strategies to stay relevant.we look forward to future research findings about 355-80-6, 2,2,3,3,4,4,5,5-Octafluoro-1-pentanol.

Reference:
Patent; Samsung SDI Co., Ltd.; Chernyshov, Denis; Shin, Woo-Cheol; Shatunov, Pavel Alexandrovich; Tereshchenko, Alexey; Egorov, Vladimir; Khasanov, Makhmut; Jeong, Myung-Hwan; EP2746288; (2014); A1;,
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