In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 3597-91-9, name is [1,1′-Biphenyl]-4-ylmethanol, the common compound, a new synthetic route is introduced below. Formula: C13H12O
In the glove box,Mn(CO)5Br (0.005 mmol),[(E)-2-(2-(1-(2-pyridyl)ethylidene)-indenyl)pyridine] (0.006 mmol),Add 1.0 mL of toluene, stir for two hours, add 2-methylquinoline 4 (2 mmol),2 g (1 mmol), after reacting at 135 C for 48 hours, the reaction was stopped and the solvent was evaporated., column chromatography ethyl acetate / petroleum ether (1:10),The trans-disubstituted olefin derivative 3ag. The product was a white solid with a yield of 92%.
The synthetic route of 3597-91-9 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Qingdao University of Science and Technology; Zhang Chunyan; (19 pag.)CN108250153; (2018); A;,
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