The major producers of chemicals have been the Europe, Japan and China. Due to the growing call for a cleaner, greener environment, people will have to find innovative ways to maintain their relevance. Here is a compound 2425-41-4, name is (2-Phenyl-1,3-dioxane-5,5-diyl)dimethanol. This compound has unique chemical properties. The synthetic route is as follows. Application In Synthesis of (2-Phenyl-1,3-dioxane-5,5-diyl)dimethanol
(8) A mixture of 2-phenyl-5,5-dihydroxymethyl-1,3-dioxane (2.2 g, 0.01 mol)4-nitrophthalonitrile (1.73 g, O. Olmol),Potassium carbonate (6.9 g, 0.05 mol)Add N, N-dimethylformamide, 50 mL; (9) The reaction was heated at 80 C for 12 hours;(10) After the reaction was stopped, the potassium carbonate was filtered off, the solvent was removed,Column chromatography using methanol / dichloromethane = 1/200 phase gave a white solid which was recrystallized from n-hexane / methylene chloride in a yield of 42%
With the rapid development of chemical substances, we look forward to future research findings about 2425-41-4.
Reference:
Patent; Shandong University , Weihai; BAI, MING; LU, RAN; WAN, PEIHONG; (8 pag.)CN104557949; (2016); B;,
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