In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 17849-38-6, name is 2-Chlorobenzyl alcohol, the common compound, a new synthetic route is introduced below. Recommanded Product: 2-Chlorobenzyl alcohol
General procedure: To a mixture of alcohol (1.0 mmol) and KI (1.5 mmol, 0.25 g) in acetonitrile (5 mL), P2O5 (1.5 mmol, 0.23 g) was added and the reaction stirred at room temperature for the time specified in Table 2. After reaction completion (TLC or GC), the reaction mixture was filtered and the residue washed with ethyl acetate (3 × 8 mL). The combined organic layers were washed with an aqueous solution of Na2S2O3 (10%, 10 mL), water (10 mL), and dried over Na2SO4. The solvent was removed under reduced pressure to afford the corresponding product. If necessary, further purification was performed by column chromatography.
The synthetic route of 17849-38-6 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Khazdooz, Leila; Zarei, Amin; Aghaei, Hamidreza; Azizi, Ghobad; Gheisari, Mohammad Mehdi; Tetrahedron Letters; vol. 57; 2; (2016); p. 168 – 171;,
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