Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps,and cheap raw materials. 110-73-6, name is 2-(Ethylamino)ethanol. A new synthetic method of this compound is introduced below., Application In Synthesis of 2-(Ethylamino)ethanol
Reference Example 19 tert-Butyl ethyl(2-hydroxyethyl)carbamate (0438) (0439) To a mixture of 2-(ethylamino)ethanol (8.91 g) and ethyl acetate (100 mL) was added di-tert-butyl dicarbonate (21.8 g) under ice-cooling. After stirring at room temperature for 3 days, the mixture was washed with saturated brine (100 mL), and dried over anhydrous magnesium sulfate. Concentration under reduced pressure gave the title compound (19.0 g) as a colorless oil. (0440) 1H-NMR (CDCl3): 1.11 (3H, t, J=7.0 Hz), 1.47 (9H, s), 3.27 (2H, q, J=7.0 Hz), 3.37 (2H, t, J=5.2 Hz), 3.73 (2H, q, J=5.2 Hz).
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Reference:
Patent; TAKEDA PHARMACEUTICAL COMPANY LIMITED; AKIYAMA, Yohko; KURASAWA, Takashi; BANDO, Hiroto; NAGAHARA, Naoki; (88 pag.)US2016/128945; (2016); A1;,
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