Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 33524-31-1, name is (2,5-Dimethoxyphenyl)methanol. This compound has unique chemical properties. The synthetic route is as follows. Product Details of 33524-31-1
2,5-dimethoxybenzyl alcohol (1.68 g, 10 mmol) was dissolved in 50 mLAnhydrous methylene chloride, stirred for 10 minutes in an ice bath,Phosphorus tribromide (1.0 g, 3.7 mmol) was slowly added dropwise,After the addition was complete, continue to react for 1 hour under ice bath.The reaction mixture was diluted with 200 mL of methylene chloride and washed with water (50 mL × 3)Saturated brine (100 mL × 1), dried over anhydrous sodium sulfate, filtered,After the solvent was evaporated to dryness under reduced pressure, the crude product was purified by column chromatography2,5-dimethoxybenzyl bromide (2.2 g, 96% yield).
If you are interested in these compounds, you can also browse my other articles.Thank you for taking the time to read this article. I hope you enjoyed it, 33524-31-1, (2,5-Dimethoxyphenyl)methanol.
Reference:
Patent; Beijing Zhuokai Biological Co., Ltd.; Xie Zuolei; (46 pag.)CN107353239; (2017); A;,
Alcohol – Wikipedia,
Alcohols – Chemistry LibreTexts